Unsuccessful synthesis of individual 1,1-dinitroethene

 

Jowita Kras ⁽¹⁾, Maria Mikulska ⁽¹⁾, Radwan Allnajar ⁽²⁾, Karolina Kula ^(1)*

⁽¹⁾ Department of Organic Chemistry and Technology, Cracow University of Technology, Warszawska 24, 31-155 Cracow (Poland),
⁽²⁾ PharmD, Faculty of Pharmacy, Libyan International Medical University, Benghazi, Libya
* Correspondence to: karolina.kula@pk.edu.pl

Pages 9-13

 

 

The possibility of the preparation of free 1,1-dinitroethene was examined experimentally on the basis of procedures described earlier for other examples of 1-R-1-nitroethenes. It was found, that these types of protocols are non-usable for the preparation of the title compound due to its high reactivity and tendency to decomposition and oligomerization.